3-(3-Chloro-benzylamino)-phthalic acid dimethyl ester → 3-(3-Chloro-benzylamino)-phthalic acid

HRID 10040

反応式

HRID 10040 の反応式
C[O:2][C:3](=[O:23])[C:4]1[C:5](=[C:10]([NH:14][CH2:15][C:16]2[CH:21]=[CH:20][CH:19]=[C:18]([Cl:22])[CH:17]=2)[CH:11]=[CH:12][CH:13]=1)[C:6]([O:8]C)=[O:7].COCCNC1C=CC=C(C(O)=O)C=1C(O)=O>>[Cl:22][C:18]1[CH:17]=[C:16]([CH:21]=[CH:20][CH:19]=1)[CH2:15][NH:14][C:10]1[CH:11]=[CH:12][CH:13]=[C:4]([C:3]([OH:23])=[O:2])[C:5]=1[C:6]([OH:8])=[O:7]

参加物

3

反応物 2

HCID 210401353-(3-Chloro-benzylamino)-phthalic acid dimethyl esterHCID 219885193-(2-Methoxy-ethylamino)-phthalic acid

生成物 1

HCID 219886073-(3-Chloro-benzylamino)-phthalic acid

実験手順

3-(3-Chloro-benzylamino)-phthalic acid dimethyl ester (1.61 g, 4.8 mmol) was treated in the same manner as described above for the synthesis of 3-(2-methoxy-ethylamino)-phthalic acid. The product of the reaction, which contained a mixture of diacid and monomethyl esters, was used without further purification.

後処理

  1. customThe product of the reaction, which
  2. customwas used without further purification

出典と根拠

ORDレコード
ord-f6f26e92084842f196349d3229d1ff9b
出典データセット
uspto-grants-2006_08
特許番号
US07091353B2

関連ノート

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