化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Melamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Melamine | HCID 7955 | — |
| 反応物 | Chlorine | HCID 24526 | — |
| 反応物 | Dimethyl ester phosphorous acid | HCID 94853 | — |
| 生成物 | Melamine | HCID 7955 | — |
| 生成物 | Dimethyl phosphite diethyl phosphate | HCID 131721781 | — |
反応手順
100 gms of dimethyl hydrogen phosphite and 25 gms of phosphorus oxytrihalide are mixed and reacted then 15 gms of ethyl alcohol are added and reacted. Cl2 and HCl evolves from the mixture. 50 gms of melamine are added then heated to 150°-200° C. while agitating for about 30 minutes, thereby producing a melamine salt of dimethyl phosphite-diethyl phosphate. The mixture is then cooled and the solid is pulverized into a powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06054515 |
| 出典データセット | uspto-grants-2000_04 |
| ORD ID | ord-e961fd3f346949ecb1dd0a5b700f1036 |
| 出典メモ | uspto-grants-2000_04 |