2-Bromopropane → HCID 53928345、化合物

反応式

[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:15])[CH2:9][N:10]2[CH:14]=[N:13][CH:12]=[N:11]2)=[CH:4][CH:3]=1.[CH:16](Br)([CH3:18])[CH3:17]>>[C:2]1([CH3:1])[CH:7]=[CH:6][C:5]([C:8]([O:15][CH:16]([CH3:18])[CH3:17])=[CH:9][N:10]2[CH:14]=[N:13][CH:12]=[N:11]2)=[CH:4][CH:3]=1

参加物

反応物 2

HCID 63582-Bromopropane

HCID 7393711-(4-methylphenyl)-2-(1h-1,2,4-triazol-1-yl)ethanone

生成物 1

HCID 53928345HCID 53928345、化合物

実験手順

Analogously to Example 1a,b, after reacting 1-(4-methylphenyl)-2-[1,2,4]triazol-1-yl-ethanone with isopropyl bromide there was obtained 1-[2-(4-tolyl)-2-isopropoxy-vinyl]-1H-[1,2,4]triazole. After reaction with HCl in dioxan there was obtained a salt of the composition C14H17N3O.HCl.[M+H]+ =243.

出典と根拠

ORDレコード: ord-59aa1ea6c89f487e9638926dabf79690
出典データセット: uspto-grants-2000_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06054588

反応ノート

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