1,1-Dimethylhydrazine → 2-(4-Methylvaleryl)furan dimethylhydrazone
反応式
[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][C:5]([C:7]1[O:8][CH:9]=[CH:10][CH:11]=1)=O.[CH3:13][N:14]([CH3:16])[NH2:15]>CCO>[CH3:13][N:14]([CH3:16])[N:15]=[C:5]([C:7]1[O:8][CH:9]=[CH:10][CH:11]=1)[CH2:4][CH2:3][CH:2]([CH3:12])[CH3:1]参加物
4
実験手順
A solution of 2-(4-methylvaleryl)furan (1 mmol) and N,N-dimethylhydrazine (1.5 mmol) in EtOH was heated at reflux for 24 h. Evaporation and distilation gave 2-(4-methylvaleryl)furan dimethylhydrazone as a brown oil.
後処理
- temperatureat reflux for 24 h
- customEvaporation and distilation
出典と根拠
- ORDレコード
- ord-5c43bbb87c0c410f80aa0de17ced7569
- 出典データセット
- uspto-grants-2000_04
- 特許番号
- US06054587
反応ノート
読み込み中…