Methyl 4-[(acetylsulfanyl)methyl]oxane-4-carboxylate → 1-Acetylsulfanylmethylcyclohexanecarboxylic acid methyl ester

HRID 1005885

反応式

HRID 1005885 の反応式
[CH3:1][O:2][C:3]([C:5]1([CH2:11][S:12][C:13](=[O:15])[CH3:14])[CH2:10][CH2:9]O[CH2:7][CH2:6]1)=[O:4].[CH3:16]OC(C1(CI)CCCCC1)=O>>[CH3:1][O:2][C:3]([C:5]1([CH2:11][S:12][C:13](=[O:15])[CH3:14])[CH2:10][CH2:9][CH2:16][CH2:7][CH2:6]1)=[O:4]

参加物

3

反応物 2

HCID 23448262Methyl 4-[(acetylsulfanyl)methyl]oxane-4-carboxylateHCID 58947958Methyl 1-(iodomethyl)cyclohexanecarboxylate

生成物 1

HCID 589479501-Acetylsulfanylmethylcyclohexanecarboxylic acid methyl ester収率 92%

実験手順

Prepared according to the method for the preparation of 4-acetylsulfanylmethyltetrahydropyran-4-carboxylic acid methyl ester, from 1-iodomethylcyclohexanecarboxylic acid methyl ester (20 g), to yield the title compound as a brown gum (15 g, 92%).

後処理

  1. customPrepared

出典と根拠

ORDレコード
ord-5768a0c849eb41108867a175c460d01f
出典データセット
uspto-grants-2004_09
特許番号
US06787536B2

関連ノート

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