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Cyclohexyl isocyanate → Octylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexyl isocyanate | HCID 18502 | — |
| 反応物 | Hydrogenated mdi | HCID 21202 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | Octylamine | HCID 8143 | 220% |
反応手順
According to the procedure described in Example 1, starting from 10 g (38.12 mmol) of methylene-bis(4-cyclohexylisocyanate), alias 4,4A′-methylene-bis(cyclohexyl isocyanate, into 200 ml of THF and 10.82 g (83.86 mmol) of octylamine into 100 ml of THF, 16.30 g of a white solid are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06790885B2 |
| 出典データセット | uspto-grants-2004_09 |
| ORD ID | ord-c3834f0705f643f18826c74abe6b1fd5 |
| 出典メモ | uspto-grants-2004_09 |