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HRID 1006875作成日:2026年10月27日

Urea → 1,3(2H,4H)-isoquinolinedione

https://huagongshe.com/reaction/1006875

反応式

関与物質

役割名称HCID仕込み量
反応物UreaHCID 1176—
反応物Homophthalic anhydrideHCID 12801—
溶媒WaterHCID 962—
生成物1,3(2H,4H)-isoquinolinedioneHCID 34943552.8%

反応手順

Homophthalic anhydride (20 g) and urea (60 g) were reacted at 170° C. for 1 hr. The reaction mixture was cooled, water (500 ml) was added thereto, and then the resulting precipitates were collected by filtration. The precipitate were washed with water and dried in hot air, to give 10.5 g of homophthalimide as a white powder.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06790844B2
出典データセットuspto-grants-2004_09
ORD IDord-eed351f54faa42abad5759f85dee4ab7
出典メモuspto-grants-2004_09