化工社化工社 化学情報印刷レポート · 研究参考用
Urea → 1,3(2H,4H)-isoquinolinedione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Urea | HCID 1176 | — |
| 反応物 | Homophthalic anhydride | HCID 12801 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 1,3(2H,4H)-isoquinolinedione | HCID 349435 | 52.8% |
反応手順
Homophthalic anhydride (20 g) and urea (60 g) were reacted at 170° C. for 1 hr. The reaction mixture was cooled, water (500 ml) was added thereto, and then the resulting precipitates were collected by filtration. The precipitate were washed with water and dried in hot air, to give 10.5 g of homophthalimide as a white powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06790844B2 |
| 出典データセット | uspto-grants-2004_09 |
| ORD ID | ord-eed351f54faa42abad5759f85dee4ab7 |
| 出典メモ | uspto-grants-2004_09 |