化工社化工社 化学情報印刷レポート · 研究参考用
Nitric Acid → HCID 86588302、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | Sulfamethoxazole | HCID 5329 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | HCID 86588302 | HCID 86588302 | 60% |
反応手順
The compound is prepared by starting from a Sulfamethoxazole solution (2 g, 7.9 mmoli) in methanol (100 ml), addition of a 65% nitric acid solution (0.500 ml) in acetonitrile (5 ml), following the procedure reported in Example 5. Sulfamethoxazole nitrate as amorphous solid is obtained. Yield 60%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06794372B2 |
| 出典データセット | uspto-grants-2004_09 |
| ORD ID | ord-7e868392ac6d4e0dbe7cd7f6fb4e6bd2 |
| 出典メモ | uspto-grants-2004_09 |