4-Ethoxy-2-nitroaniline → 6-Chloro-N-(4-ethoxy-2-nitrophenyl)-3-pyridinecarboxamide

HRID 1007184

反応式

HRID 1007184 の反応式
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][N:3]=1.[CH2:11]([O:13][C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[C:16]([N+:21]([O-:23])=[O:22])[CH:15]=1)[CH3:12]>>[Cl:1][C:2]1[N:3]=[CH:4][C:5]([C:6]([NH:18][C:17]2[CH:19]=[CH:20][C:14]([O:13][CH2:11][CH3:12])=[CH:15][C:16]=2[N+:21]([O-:23])=[O:22])=[O:7])=[CH:9][CH:10]=1

参加物

3

反応物 2

HCID 692294-Ethoxy-2-nitroanilineHCID 27821656-Chloronicotinoyl Chloride

生成物 1

HCID 98401276-Chloro-N-(4-ethoxy-2-nitrophenyl)-3-pyridinecarboxamide

実験手順

The title compound was prepared from 6-chloronicotinoyl chloride and 4-ethoxy-2-nitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.13 (s, 1H), 9.01 (d, J=2.4, 1H), 8.82 (d, J=9.3, 1H), 8.24-8.20 (m, 1H), 7.74 (d, J=3.0, 1H), 7.51 (d, J=7.8, 1H), 7.34-7.30(m, 1H), 4.11 (q, J=6.9, 2H), 1.47 (t, J=6.9, 3H).

後処理

  1. customwas obtained as a yellow solid

出典と根拠

ORDレコード
ord-49b35d11275d4122a82d2d99e7daf1dd
出典データセット
uspto-grants-2004_09
特許番号
US06794397B2

関連ノート

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