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2,4-Dinitroaniline → 6-Chloro-N-(2,4-dinitrophenyl)-3-pyridinecarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,4-Dinitroaniline | HCID 7321 | — |
| 反応物 | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| 生成物 | 6-Chloro-N-(2,4-dinitrophenyl)-3-pyridinecarboxamide | HCID 22668935 | — |
反応手順
The title compound was prepared from 6-chloronicotinoyl chloride and 2,4-dinitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.69 (bs, 1H), 9.28-9.23 (m, 2H), 9.06-9.05 (m, 1H), 8.61-8.57 (m, 1H), 8.28-8.24 (m, 1H), 7.59-7.56 (m, 1H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06794397B2 |
| 出典データセット | uspto-grants-2004_09 |
| ORD ID | ord-9467038bc9184c648988a41feae5a4d7 |
| 出典メモ | uspto-grants-2004_09 |