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4-Ethoxy-2-nitroaniline → N-(4-Ethoxy-2-nitrophenyl)-6-methylnicotinamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Ethoxy-2-nitroaniline | HCID 69229 | — |
| 反応物 | 6-Methylnicotinic acid | HCID 137860 | — |
| 生成物 | N-(4-Ethoxy-2-nitrophenyl)-6-methylnicotinamide | HCID 9817832 | — |
反応手順
The title compound was prepared from 6-methylnicotinic acid and 4-ethoxy-2-nitroaniline and was obtained as a yellow solid as described in Example 15. 1H NMR (CDCl3): 11.09 (s, 1H), 9.12 (d, J=2.1, 1H), 8.85 (d, J=9.3, 1H), 8.16-8.13 (m, 1H), 7.73 (d, J=3.0, 1H), 7.34-7.29 (m, 2H), 4.11 (q, J=6.9, 2H), 2.67 (s, 3H), 1.46 (t, J=6.9, 3H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06794397B2 |
| 出典データセット | uspto-grants-2004_09 |
| ORD ID | ord-02dc02652dd84537b65dea3f788004c2 |
| 出典メモ | uspto-grants-2004_09 |