Methylselenocysteine → HCID 131724597、化合物

HRID 1007629ノート

反応式

HRID 1007629 の反応式
C[Se:2][CH2:3][C@H:4]([NH2:8])[C:5]([OH:7])=[O:6].Cl.[CH3:10]OC(=O)[C@H](C)N[Cl:15].Cl.ClN[C@H](C(O)=O)C.ClN[C@H](C(O)=O)C.C[Se]>CO>[ClH:15].[CH3:10][NH:8][C@H:4]([C:5]([OH:7])=[O:6])[CH2:3][SeH:2]

参加物

7

反応物 5

HCID 147004MethylselenocysteineHCID 63270006486-05-1HCID 13743744N-Chloro-L-alanineHCID 22871751HCID 22871751、化合物HCID 88052998HCID 88052998、化合物

生成物 1

HCID 131724597HCID 131724597、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

A process for manufacturing L-Se-methylselenocysteine by reaction of chloroalanine methyl ester hydrochloride or chloroalanine hydrochloride or chloroalanine with methylselenol or its salts in a solvent, acidifying the reaction mixture after completion of reaction, isolating methyselenocysteine hydrochloride as a methanol solution, neutralizing the methanol solution with triethyl amine to precipitate L-Se-methylselenocysteine.

後処理

  1. customafter completion of reaction

出典と根拠

ORDレコード
ord-3fa4da69c54a4e3ba1620aa1e14c3c1d
出典データセット
uspto-grants-2004_09
特許番号
US06794537B1

反応ノート

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