反応式
[CH3:1][N:2]([C:4]1[CH:9]=[CH:8][C:7]([N:10]=[N:11][C:12]2[CH:17]=[CH:16][C:15]([S:18](Cl)(=[O:20])=[O:19])=[CH:14][CH:13]=2)=[CH:6][CH:5]=1)[CH3:3].[NH2:22][CH2:23][CH2:24][O:25][CH2:26][CH2:27][N:28]1[C:36]2[C:35]([CH3:37])=[C:34]([CH3:38])[N:33]=[C:32]([NH2:39])[C:31]=2[N:30]=[C:29]1[CH3:40]>>[NH2:39][C:32]1[C:31]2[N:30]=[C:29]([CH3:40])[N:28]([CH2:27][CH2:26][O:25][CH2:24][CH2:23][NH:22][S:18]([C:15]3[CH:16]=[CH:17][C:12]([N:11]=[N:10][C:7]4[CH:8]=[CH:9][C:4]([N:2]([CH3:3])[CH3:1])=[CH:5][CH:6]=4)=[CH:13][CH:14]=3)(=[O:20])=[O:19])[C:36]=2[C:35]([CH3:37])=[C:34]([CH3:38])[N:33]=1参加物
3
実験手順
Using the method of Examples 34-50, 4-dimethylaminoazobenzene-4′-sulfonyl chloride was reacted with 1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The product was purified using Method A. The observed accurate mass was 551.2551.
出典と根拠
- ORDレコード
- ord-ed438f9a29814fdc884b2a8488d2fbd9
- 出典データセット
- uspto-grants-2004_09
- 特許番号
- US06797718B2
関連ノート
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