Hydrochloric Acid → HCID 54402950、化合物

HRID 1010522ノート

反応式

HRID 1010522 の反応式
C([O:3][C:4](=[O:13])[CH2:5][N:6]1[CH:10]=[C:9]([CH2:11][CH3:12])[N:8]=[CH:7]1)C.Cl>>[CH2:11]([C:9]1[N:8]=[CH:7][N:6]([CH2:5][C:4]([OH:13])=[O:3])[CH:10]=1)[CH3:12]

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 57731307HCID 57731307、化合物

生成物 1

HCID 54402950HCID 54402950、化合物

実験手順

1.7 g (9.5 mmol) of (4-ethyl-imidazol-1-yl)-acetic acid ethyl ester are dissolved in 47 ml (190 mmol) 4N HCl and the mixture is heated to reflux. After 2 h the mixture is cooled to rt and the solvent is removed in vacuo. The resulting product is used without further purification.

後処理

  1. temperaturethe mixture is heated to reflux
  2. customthe solvent is removed in vacuo
  3. customThe resulting product is used without further purification

出典と根拠

ORDレコード
ord-bb57c63f9b0d41b99bff4471bff17847
出典データセット
uspto-grants-2011_07
特許番号
US07977323B2

反応ノート

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