化工社化工社 化学情報印刷レポート · 研究参考用
3-(Diethylamino)pyrrolidine → [5-(3-bromo-phenyl)-1,4-dimethyl-1H-pyrazol-3-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(Diethylamino)pyrrolidine | HCID 19961995 | — |
| 反応物 | 5-(3-bromo-phenyl)-1,4-dimethyl-1H-pyrazole-3-carboxylic acid | HCID 67315328 | — |
| 生成物 | [5-(3-bromo-phenyl)-1,4-dimethyl-1H-pyrazol-3-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone | HCID 67315151 | 94% |
反応手順
In analogy to the procedure described in example 12D], 5-(3-bromo-phenyl)-1,4-dimethyl-1H-pyrazole-3-carboxylic acid and 3-(diethylamino)pyrrolidine gave the title compound in 94% yield as white needles. MS: 419.2 (MH+, 1 Br).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07977358B2 |
| 出典データセット | uspto-grants-2011_07 |
| ORD ID | ord-289c11f5102c4cb2ae58ef35805e8b61 |
| 出典メモ | uspto-grants-2011_07 |