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2,3-Dihydro-1,4-benzodioxin-6-carbaldehyde → HCID 178489238、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dihydro-1,4-benzodioxin-6-carbaldehyde | HCID 248127 | — |
| 反応物 | 4-Methoxy-1,3-benzothiazole | HCID 12631858 | — |
| 反応物 | HCID 178502731 | HCID 178502731 | — |
| 生成物 | HCID 178489238 | HCID 178489238 | — |
反応手順
Using 4-methoxy-benzothiazole (5 mmol), [trans-4-(methoxy-methyl-carbamoyl)-cyclohexyl]-carbamic acid tert-butyl ester (2.5 mmol) and 2,3-dihydro-benzo[1,4]dioxine-6-carbaldehyde (0.3 mmol) according to the same protocol as that described for example 1, steps 1.a to 1.c, the title compound was obtained as a off-white solid (41 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07981886B2 |
| 出典データセット | uspto-grants-2011_07 |
| ORD ID | ord-c37facaf906446528f955f588c4ba5d6 |
| 出典メモ | uspto-grants-2011_07 |