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HRID 1014963作成日：2026年10月26日

2-(1-Methyl-1H-imidazol-4-yl)ethanamine bis(4-methylbenzenesulfonate) → 1-Methylhistamine

https://huagongshe.com/reaction/1014963

反応式

関与物質

役割名称HCID仕込み量
反応物2-(1-Methyl-1H-imidazol-4-yl)ethanamine bis(4-methylbenzenesulfonate)HCID 86254824—
溶媒WaterHCID 962—
生成物1-MethylhistamineHCID 3614—

反応手順

[2-(1-methyl-1H-imidazol-4-yl)ethyl]amine bis(4-methylbenzenesulfonate) (50 g) was dissolved in IMS (200 ml)/water (200 ml). This was passed through a DOWEX550A column (600 g), eluting with IMS (ca. 4 litres). Appropriate fractions were combined and concentrated in vacuo to yield the title compound, 13.4 g.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07985740B2
出典データセットuspto-grants-2011_07
ORD IDord-f3da4045887c466dbdc32a66a7e10fda
出典メモuspto-grants-2011_07