o-Chlorophenylhydrazine hydrochloride → 2-Chloro-6-(2-chlorophenylhydrazino)-9-cyclopentylpurine

HRID 1017293

反応式

HRID 1017293 の反応式
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4](Cl)[N:3]=1.[Cl:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=1[NH:24][NH2:25]>C(N(CC)CC)C>[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4]([NH:25][NH:24][C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=2[Cl:17])[N:3]=1

参加物

4

反応物 2

HCID 418422o-Chlorophenylhydrazine hydrochlorideHCID 108011162,6-dichloro-9-cyclopentyl-9H-purine

生成物 1

HCID 542173722-Chloro-6-(2-chlorophenylhydrazino)-9-cyclopentylpurine

試薬・触媒・溶媒 1

HCID 8471Triethylamine溶媒

実験手順

2-Chloro-6-(2-chlorophenylhydrazino)-9-cyclopentylpurine is prepared from 2,6-dichloro-9-cyclopentylpurine, 2-chlorophenylhydrazine, and triethylamine essentially as described above in Example 1, Scheme A, step b.

出典と根拠

ORDレコード
ord-a1b28222c1fb49bea1e5290bb76c7dcf
出典データセット
uspto-grants-2002_11
特許番号
US06479487B1

関連ノート

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