化工社化工社 化学情報印刷レポート · 研究参考用
Aluminum(III) Chloride → 4-Iodo-3-nitro-benzophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 反応物 | 4-Iodo-3-nitrobenzoic acid | HCID 11208598 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 4-Iodo-3-nitro-benzophenone | HCID 11187302 | — |
反応手順
5.3 g (17 mmol) of 4-iodo-3-nitrobenzoic acid and 8.0 g (60 mmol) of aluminium trichloride are added successively to 70 ml of benzene while cooling with an ice bath. Then the mixture is stirred for 2 hours at ambient temperature, then poured into ice water, extracted with methylene chloride, dried with sodium sulphate and concentrated in vacuo.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06479524B1 |
| 出典データセット | uspto-grants-2002_11 |
| ORD ID | ord-2af6b35e3597405292621887034b7779 |
| 出典メモ | uspto-grants-2002_11 |