Potassium Hydroxide → HCID 19901125、化合物
反応式
[S:1]1[CH2:4][S:3][C:2]1=[C:5]([C:11]([O:13]CC)=[O:12])[C:6]([O:8][CH2:9][CH3:10])=[O:7].[OH-].[K+]>C(O)C>[S:1]1[CH2:4][S:3][C:2]1=[C:5]([C:11]([OH:13])=[O:12])[C:6]([O:8][CH2:9][CH3:10])=[O:7]参加物
4
実験手順
Diethyl 2-(1,3-dithietan-2-ylidene)malonate was treated with a solution of potassium hydroxide in ethanol. The resultant solid was isolated and purified by the same method as in Example 1 to afford the titled compound as a white solid. (51%).
後処理
- customThe resultant solid was isolated
- custompurified by the same method as in Example 1
出典と根拠
- ORDレコード
- ord-192d02d1cbd44f0e857d2f19aac69229
- 出典データセット
- uspto-grants-1992_04
- 特許番号
- US05103013
反応ノート
読み込み中…