化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Hydroxide → Isopropyl 2-(1,3-dithiolan-2-ylidene)-2-carboxyacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Isoprothiolane | HCID 39681 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | Isopropyl 2-(1,3-dithiolan-2-ylidene)-2-carboxyacetate | HCID 19901144 | — |
反応手順
Diisopropyl 2-(1,3-dithiolan-2-ylidene)malonate was treated with a solution of potassium hydroxide in isopropyl alcohol. The resultant solid was isolated and purified by the same method as in Example 1 to afford the titled compound as a white solid. (64%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05103013 |
| 出典データセット | uspto-grants-1992_04 |
| ORD ID | ord-0ed5ad2b78c74541b0ad936cbb789840 |
| 出典メモ | uspto-grants-1992_04 |