反応式
O[C:2]1[CH:7]=[C:6]([O:8][CH2:9][O:10][CH3:11])[CH:5]=[C:4](OCOC)[C:3]=1[C:16](=[O:18])C>C(O)C>[CH3:6][O:8][CH2:9][O:10][C:5]1[CH:4]=[C:3]([CH:2]=[CH:7][C:6]=1[O:8][CH2:9][O:10][CH3:11])[CH:16]=[O:18]参加物
3
実験手順
In 260 ml of ethanol were dissolved 33.37 g of the 2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone obtained in Production Example 11 and 32.20 g of the 3,4-bis(methoxymethoxy)benzaldehyde obtained in Production Example 24, and 300 ml of a saturated solution of potassium hydroxide in ethanol was added to the solution and the mixture was stirred for 24 hours to effect a reaction. After the reaction, the pH value of the reaction liquid was adjusted to about 6 by 6N hydrochloric acid, and the formed precipitate was recovered by filtration, washed with water and dried to obtain 53.17 g (yield=87.9%) of 2'-hydroxy-3,4,4',6'-tetrakis(methoxymethoxy)chalcone.
出典と根拠
- ORDレコード
- ord-ab4fe7a5970b4393aba04cc2d4a14e60
- 出典データセット
- uspto-grants-1992_04
- 特許番号
- US05106871
関連ノート
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