1-Chloro-5-hydroxy-5-methylhexane → 7-Butyl-3-ethyl-1-(5-hydroxy-5-methylhexyl)-xanthine

反応式

[CH2:1]([N:5]1[C:13]2[C:12](=[O:14])[NH:11][C:10](=[O:15])[N:9]([CH2:16][CH3:17])[C:8]=2[N:7]=[CH:6]1)[CH2:2][CH2:3][CH3:4].Cl[CH2:19][CH2:20][CH2:21][CH2:22][C:23]([OH:26])([CH3:25])[CH3:24]>>[CH2:1]([N:5]1[C:13]2[C:12](=[O:14])[N:11]([CH2:19][CH2:20][CH2:21][CH2:22][C:23]([OH:26])([CH3:25])[CH3:24])[C:10](=[O:15])[N:9]([CH2:16][CH3:17])[C:8]=2[N:7]=[CH:6]1)[CH2:2][CH2:3][CH3:4]

参加物

反応物 2

HCID 137476791-Chloro-5-hydroxy-5-methylhexane

HCID 184608567-Butyl-3-ethylxanthine

生成物 1

HCID 198196487-Butyl-3-ethyl-1-(5-hydroxy-5-methylhexyl)-xanthine

実験手順

According to Example 1 7-butyl-3-ethylxanthine was reacted with 1-chloro-5-hydroxy-5-methylhexane; after isolation the final product was recrystallized from a mixture of ethyl acetate and petroleum ether.

後処理

customafter isolation the final product was recrystallized from a mixture of ethyl acetate and petroleum ether

出典と根拠

ORDレコード: ord-d1efd08756124e60a8f51d0b2eb05c1b
出典データセット: uspto-grants-1992_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05109003

反応ノート

読み込み中…

参加物