化工社化工社 化学情報印刷レポート · 研究参考用
Barium nitrate → Sulfate Ion
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Barium nitrate | HCID 24798 | — |
| 反応物 | Perchlorate | HCID 123351 | — |
| 反応物 | Hydroxylamine, sulfate (1:1) | HCID 159255 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 反応物 | Calcium | HCID 5460341 | — |
| 生成物 | Sulfate Ion | HCID 1117 | — |
| 生成物 | Hydroxylamine, perchlorate (1:1) | HCID 167307 | — |
| 生成物 | Hydroxylammonium nitrate | HCID 10129901 | — |
反応手順
In the aqueous precipitation process, a saturated aqueous solution of hydroxylamine sulfate is combined with a saturated aqueous solution of sodium, calcium or barium nitrate or perchlorate. These reactions result in the formation of a very difficult-to-filter sulfate precipitate and of an aqueous solution of either hydroxylamine nitrate (HAN) or hydroxylamine perchlorate (HAP). In the case of HAN, the concentration is about 15%. Since most of the useful concentrations of these oxidizers are in the 50 to 85% range water has to be removed by the costly process of distillation. Because the sulfate is difficult to precipitate, residual metal contaminants are present in high concentrations in the final product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04954328 |
| 出典データセット | uspto-grants-1990_09 |
| ORD ID | ord-a429a5b3425a4bd4bba7641e67b534bd |
| 出典メモ | uspto-grants-1990_09 |