1,4-Dioxane hydrochloride → HCID 13689669、化合物
反応式
C(OC(NC[C@H]1CC[C@H]([C:16]([NH:18][C:19](=[O:29])[C@H:20]([CH2:22][C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)[NH2:21])=O)CC1)=O)(C)(C)C.[ClH:30].O1CCOCC1>>[ClH:30].[CH3:16][NH:18][C:19](=[O:29])[C@H:20]([CH2:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1)[NH2:21]参加物
3
実験手順
To the compound (I) (2.00 g), 4N hydrogen chloride/1,4-dioxane solution (36 ml) was added, and the mixture was stirred under room temperature for one hour. The solvent was evaporated under a reduced pressure and toluene was added to the residue, followed by reevaporation to give L-phenylalanine methylamide hydrochloride quantitatively as a white powder.
後処理
- customThe solvent was evaporated under a reduced pressure and toluene
- additionwas added to the residue
- customfollowed by reevaporation
出典と根拠
- ORDレコード
- ord-25d45ab4575f448893b75d75b5648a25
- 出典データセット
- uspto-grants-1990_09
- 特許番号
- US04954512
反応ノート
読み込み中…