化工社化工社 化学情報印刷レポート · 研究参考用
Water → 1,1'-(Dithiodicarbonothioyl)bis(4-methylpiperazine)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Carbon Disulfide | HCID 6348 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 1-Methylpiperazine | HCID 53167 | — |
| 触媒 | Potassium ferricyanide | HCID 26250 | — |
| 生成物 | 1,1'-(Dithiodicarbonothioyl)bis(4-methylpiperazine) | HCID 30054 | — |
反応手順
5 parts of N-methylpiperazine are reacted in 100 parts of water with 2 parts of sodium hydroxide and 4.2 parts of carbon disulfide and oxidized with 16.5 parts of potassium hexacyanoferrate(III). Obtained are 8.6 parts of the compound with 41.1% C, 6.5% H, and 15.7% N (calculated: 41.1% C, 6.3% H, 16.0% N, 36.6% S).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04956433 |
| 出典データセット | uspto-grants-1990_09 |
| ORD ID | ord-d62a17d3cd924e699fc26ff9dad7e5fb |
| 出典メモ | uspto-grants-1990_09 |