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2-(7-nitro-1H-indazol-4-yl)acetonitrile → 2-(3-Methoxy-4-nitrophenyl)acetonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(7-nitro-1H-indazol-4-yl)acetonitrile | HCID 13629308 | — |
| 反応物 | N,N-Dimethyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amine | HCID 54285175 | — |
| 生成物 | 2-(3-Methoxy-4-nitrophenyl)acetonitrile | HCID 13629317 | 99.3% |
反応手順
19.8 g of N,N-dimethyl-N-[2-(3-methoxy-4nitrophenyl)ethenyl]amine and 30.0 g of hydroxylamineorthosulfonic acid are reacted as described in connection with preparing 2-(7-nitro-1H-indazol-4-yl)acetonitrile, thus obtaining 17.0 g of (3-methoxy-4-nitrophenyl)acetonitrile, mp 85°-86.5° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04958026 |
| 出典データセット | uspto-grants-1990_09 |
| ORD ID | ord-5e0df74fa9d84916b8697d0da74d71e9 |
| 出典メモ | uspto-grants-1990_09 |