Lithium Benzoate → HCID 12647149、化合物

HRID 1032624ノート

反応式

HRID 1032624 の反応式
Cl[CH2:2][C:3]([O-:5])=[O:4].[Li+].[C:7]([O-:15])(=[O:14])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.[Li+]>CN(C=O)C>[C:7]([O:15][CH2:2][C:3]([OH:5])=[O:4])(=[O:14])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1

参加物

4

反応物 2

HCID 2724073Lithium BenzoateHCID 23695591Lithium chloroacetate

生成物 1

HCID 12647149HCID 12647149、化合物

試薬・触媒・溶媒 1

HCID 6228Dimethylformamide溶媒

実験手順

13 g lithium chloroacetate (0.10 m) and 17.6 g lithium benzoate (0.10 m) were combined in a 250 ml R.b. flask with 50 ml DMF. This was heated on an oil bath to 110°-120° C. with magnetic stirring for 3 hrs. (The solution at first was clear, but after 2-3 hrs. a white precipitate formed).

後処理

  1. temperatureThis was heated on an oil bath to 110°-120° C.
  2. wait(The solution at first was clear, but after 2-3 hrs
  3. customa white precipitate formed)

出典と根拠

ORDレコード
ord-7f6e7517a81c49d2a89681fa27026b61
出典データセット
uspto-grants-1990_09
特許番号
US04959187

反応ノート

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