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Thionyl Chloride → 4-Decyloxybenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 4-(Decyloxy)benzoic acid | HCID 138527 | — |
| 触媒 | Dimethylformamide | HCID 6228 | — |
| 溶媒 | Carbon Tetrachloride | HCID 5943 | — |
| 生成物 | 4-Decyloxybenzoyl chloride | HCID 11779353 | — |
反応手順
A 300 ml two-necked flask equipped with a stirrer and a reflux condenser was charged with 100 ml of carbon tetrachloride, 4.5 ml of thionyl chloride and 11.1 g of 4-n-decyloxybenzoic acid obtained by a conventional method, and heated under reflux together with one drop of dimethylformamide for 4 hours. Then, unreacted thionyl chloride was removed under reduced pressure to obtain 4-decyloxybenzoyl chloride as a colorless liquid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05308536 |
| 出典データセット | uspto-grants-1994_05 |
| ORD ID | ord-de8ea2b0bfca4db4a062d4e0f3d4eec8 |
| 出典メモ | uspto-grants-1994_05 |