2-[2-(5-ethyl-2-methoxy-6-methylpyridin-3-yl)ethyl]-2,3-dihydro-1H-isoindole-1,3-dione → L 693593

反応式

C[O:2][C:3]1[C:8]([CH2:9][CH2:10][N:11]2[C:15](=[O:16])[C:14]3=[CH:17][CH:18]=[CH:19][CH:20]=[C:13]3[C:12]2=[O:21])=[CH:7][C:6]([CH2:22][CH3:23])=[C:5]([CH3:24])[N:4]=1.Cl.N1C=CC=CC=1>>[C:12]1(=[O:21])[N:11]([CH2:10][CH2:9][C:8]2[C:3](=[O:2])[NH:4][C:5]([CH3:24])=[C:6]([CH2:22][CH3:23])[CH:7]=2)[C:15](=[O:16])[C:14]2=[CH:17][CH:18]=[CH:19][CH:20]=[C:13]12

参加物

反応物 2

HCID 4642742-[2-(5-ethyl-2-methoxy-6-methylpyridin-3-yl)ethyl]-2,3-dihydro-1H-isoindole-1,3-dione

HCID 10176127Pyridinium chloride

生成物 1

HCID 65001L 693593

実験手順

2-methoxy-3-(2-phthalimidoethyl)-5-ethyl-6-methyl pyridine is heated at 150° C. for 5-10 minutes in the presence of excess pyridine hydrochloride to give the above titled product.

出典と根拠

ORDレコード: ord-5488e5277a824fe88341cc749e8a02a3
出典データセット: uspto-grants-1994_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05308854

反応ノート

読み込み中…