Hydrochloric Acid → 1H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

HRID 1033747ノート

反応式

HRID 1033747 の反応式
[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][N:2]1C(OCC)=O.[ClH:15]>>[ClH:15].[ClH:15].[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][NH:2]1

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 18953633ethyl 1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxylate

生成物 1

HCID 189536441H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

実験手順

10.4 g (51 mmol) of ethyl 2,3-dihydro-1H-pyrrolo-[3,4-c]pyridine-2-carboxylate are refluxed for 15 hours together with 100 ml of concentrated hydrochloric acid. The batch is evaporated, and the crystalline residue is stirred with acetone. The product is filtered off with suction and dried in the air.

後処理

  1. customThe batch is evaporated
  2. filtrationThe product is filtered off with suction
  3. customdried in the air

出典と根拠

ORDレコード
ord-da275ca293f44d51a9ea56983ed6266b
出典データセット
uspto-grants-1994_05
特許番号
US05312823

反応ノート

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