関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 3-(2-Methylpropenyl)benzonitrile | HCID 19024792 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 3-Isobutylbenzonitrile | HCID 19024755 | 94% |
反応手順
To a solution of 3-(2-methyl-1-propenyl)benzonitrile (5.80 g) in methanol (50 ml) was added 10% palladium on activated carbon (1 g), and the mixture was stirred under hydrogen atmosphere (3 atm) at 25° C. for 1 hour. The catalyst was filtered off and the liltrate was evaporated to give 3-isobutylbenzonitrile (5.52 g) as a pale yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05312829 |
|---|
| 出典データセット | uspto-grants-1994_05 |
|---|
| ORD ID | ord-f5fee2c5150e427682aeaa078f4e5058 |
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| 出典メモ | uspto-grants-1994_05 |
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