化工社化工社 化学情報印刷レポート · 研究参考用
Boron tribromide → 6-(4-Hydroxyphenyl)-2-naphthol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Boron tribromide | HCID 25134 | — |
| 反応物 | 2-Methoxy-6-(4-methoxyphenyl)naphthalene | HCID 11149734 | — |
| 生成物 | 6-(4-Hydroxyphenyl)-2-naphthol | HCID 11459006 | 98% |
反応手順
The compound is prepared by reaction of 2-methoxy-6-(4-methoxyphenyl)-naphthalene (150 mg, 0.57 mmol, 1 eq) with boron tribromide (3.4 ml, 3.4 mmol, 3 eq) according to method G. Purification by column chromatography with hexane/ethyl acetate 9/1 as the eluent yields the desired product in a yield of 98%, 132 mg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08546392B2 |
| 出典データセット | uspto-grants-2013_10 |
| ORD ID | ord-115a30c013ea425488c9d55d705f1b01 |
| 出典メモ | uspto-grants-2013_10 |