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HRID 1038675作成日：2026年10月27日

1,3-Dichloro-2-isocyanatobenzene → 1-(2,6-Dichloro-phenyl)-3-[6-(4-morpholin-4-yl-phenylamino)-pyrimidin-4-yl]-urea

https://huagongshe.com/reaction/1038675

反応式

関与物質

役割名称HCID仕込み量
反応物1,3-Dichloro-2-isocyanatobenzeneHCID 604537—
反応物N-(4-Morpholin-4-yl-phenyl)-pyrimidine-4,6-diamineHCID 66669896—
生成物1-(2,6-Dichloro-phenyl)-3-[6-(4-morpholin-4-yl-phenylamino)-pyrimidin-4-yl]-ureaHCID 57710274—

反応手順

The title compound is prepared analogously as described in Example 105B from N-(4-morpholin-4-yl-phenyl)-pyrimidine-4,6-diamine and 2,6-dichlorophenyl isocyanate. Faintly violet solid, HPLC: tR=3.74 min (purity: 100%, gradient F), ESI-MS: 459.3/461.3 [MH]+.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08552002B2
出典データセットuspto-grants-2013_10
ORD IDord-f908716032de4da69aa70d9be131131e
出典メモuspto-grants-2013_10