関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Tetralin | HCID 8404 | — |
| 反応物 | 2-Phenylthiophenol | HCID 2760413 | — |
| 生成物 | Biphenyl | HCID 7095 | — |
反応手順
A volume of 1.5 ml of a tetralin solution containing 0.1 M of 2-phenylthiopheol was placed into 3 ml stainless-steel mini-bomb inside a dry-box. The mini-bomb was heated at 375° C. in an oven for a certain period of time and the content analyzed by GC/MS. Results in Table 1 below indicate desulfurization of 2-phenylthiophenol, giving biphenyl as the major product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08557101B2 |
|---|
| 出典データセット | uspto-grants-2013_10 |
|---|
| ORD ID | ord-af10a4291d544822bec950361b4f5258 |
|---|
| 出典メモ | uspto-grants-2013_10 |
|---|
