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HRID 1041821作成日:2026年10月24日

1,2-Dichloroethane → 6-Amino-2-[bis(carboxymethyl)amino]hexanoic acid

https://huagongshe.com/ja/reaction/1041821

反応式

関与物質

役割名称HCID仕込み量
反応物1,2-DichloroethaneHCID 11—
反応物N-(5-Amino-1-carboxypentyl)iminodiacetic acidHCID 7019830—
溶媒Dimethyl SulfoxideHCID 679—
生成物6-Amino-2-[bis(carboxymethyl)amino]hexanoic acidHCID 2735296—

反応手順

A solution was prepared by the addition of 1 mmol of EDC and 0.2 mmol of NHS to 1 ml of DMSO, and 50 μl of the thus prepared solution was added onto the CMD film. The solution was then allowed to undergo the reaction at the room temperature for 30 minutes. After the solution was removed, washing with DMSO was performed one time. Also, a solution prepared by the addition of 0.1 mmol of AB-NTA (supplied by Dojin Kagaku K.K.) to 1 ml of DMSO was allowed to undergo the reaction for 12 hours. The solution was removed, and washing with ultra pure water was performed one time.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08557194B2
出典データセットuspto-grants-2013_10
ORD IDord-875e695d231845f9836da25fe77b3704
出典メモuspto-grants-2013_10