化工社化工社 化学情報印刷レポート · 研究参考用
4-Nitroindan → 4-Aminoindan
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Nitroindan | HCID 253578 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-Aminoindan | HCID 122569 | — |
反応手順
4-Nitro-indan (5.00 g, 30.70 mmol) was dissolved in methanol, and Pd/C (500 mg) was added. The resulting reaction mixture was hydrogenated at 50 psi for 14 hours. Filtration through celite and concentration afforded the title indan-4-yl-amine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08557853B2 |
| 出典データセット | uspto-grants-2013_10 |
| ORD ID | ord-188263aad68d460089858ec4f2183d14 |
| 出典メモ | uspto-grants-2013_10 |