3-(5-Methyl-1,2,4-oxadiazol-3-yl)phenyl acetate → 3-(5-Methyl-1,2,4-oxadiazol-3-yl)phenol
反応式
C([O:4][C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([C:11]2[N:15]=[C:14]([CH3:16])[O:13][N:12]=2)[CH:6]=1)(=O)C>Cl>[CH3:16][C:14]1[O:13][N:12]=[C:11]([C:7]2[CH:6]=[C:5]([OH:4])[CH:10]=[CH:9][CH:8]=2)[N:15]=1参加物
3
実験手順
A solution of 8.55 g (39.18 mmol) of the product obtained in Step C above in 120 ml of 1N HCl solution is heated at reflux for 90 minutes and is then left at ambient temperature overnight, with stirring. The precipitate is filtered off to yield the title product.
後処理
- temperatureat reflux for 90 minutes
- filtrationThe precipitate is filtered off
出典と根拠
- ORDレコード
- ord-10a488ae5abf4fc5897e9468539c7837
- 出典データセット
- uspto-grants-2013_10
- 特許番号
- US08569285B2
反応ノート
読み込み中…