関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Calcium chloride, dihydrate | HCID 6093260 | — |
| 反応物 | bicyclo2.2.1heptane-2,3-dicarboxylic acid, disodium salt | HCID 21981355 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Calcium bicyclo(2.2.1)heptane-2,3-dicarboxylate | HCID 21981350 | — |
反応手順
To a solution of disodium bicyclo[2.2.1]heptane-2,3-dicarboxylate (22.6 g, 0.1 mol) in water (150 g) was added a solution of calcium chloride dihydrate (14.7 g, 0.1 mol) in water (100 g). The mixture stirred at 60° C. for 2 hours. The resulting white precipitate was filtered. The white powdery product was dried and milled (m.p. >300° C.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07094820B2 |
|---|
| 出典データセット | uspto-grants-2006_08 |
|---|
| ORD ID | ord-c0156d75e2c14a898911d22916c87e2d |
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| 出典メモ | uspto-grants-2006_08 |
|---|
