HCID 23134613、化合物 → 3-Ethoxy-2-methylaniline
反応式
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([N+:10]([O-])=O)[C:5]=1[CH3:13])[CH3:2]>[C].[Pd].C(O)C>[CH2:1]([O:3][C:4]1[C:5]([CH3:13])=[C:6]([CH:7]=[CH:8][CH:9]=1)[NH2:10])[CH3:2]参加物
4
実験手順
A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.
後処理
- filtrationThe mixtures were filtered
- concentrationthe filtrates were concentrated
出典と根拠
- ORDレコード
- ord-0124a7c0ff9a437f91fc0767421e3bb0
- 出典データセット
- uspto-grants-2016_07
- 特許番号
- US09380782B2
反応ノート
読み込み中…