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Diethyl Ether → HCID 178440565、化合物

HRID 1050656
ノート
印刷プレビュー

反応式

HRID 1050656 の反応式
C1(=[C:7]2[C:19]3[C:11]([CH:12]=[C:13]4[C:18]=3[CH:17]=[C:16]([C:20]([CH3:23])([CH3:22])[CH3:21])[C:15]([C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=3)=[CH:14]4)=[C:10](C3C=CC=C3)[C:9]([C:35]3[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=3)=[C:8]2[C:41]([CH3:44])([CH3:43])[CH3:42])CCCCC1.C(O[CH2:48][CH3:49])C.[CH2:50]([Li])[CH2:51][CH2:52]C.[Cl-:55].[Cl-].[Cl-].[Cl-].[Zr+4:59].[CH3:60][CH2:61][CH2:62][CH2:63][CH2:64][CH3:65]>>[Cl-:55].[Cl-:55].[C:62]1(=[Zr+2:59]([CH:49]2[CH:48]=[CH:52][CH:51]=[CH:50]2)[C:10]2[C:11]3[CH2:12][C:13]4[C:18](=[CH:17][C:16]([C:20]([CH3:21])([CH3:22])[CH3:23])=[C:15]([C:24]5[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=5)[CH:14]=4)[C:19]=3[CH:7]=[C:8]([C:41]([CH3:44])([CH3:42])[CH3:43])[C:9]=2[C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[CH2:61][CH2:60][CH2:65][CH2:64][CH2:63]1
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

6

反応物 5

HCID 3283Diethyl EtherHCID 8058HexaneHCID 9856075Zirconium chloride (ZrCl4), (T-4)-HCID 131736075Cyclohexylidene(cyclopentadienyl)(2,7-diphenyl-3,6-ditert-butylfluorene)HCID 178418339Butyllithium

生成物 1

HCID 178440565HCID 178440565、化合物収率 57%

反応条件

温度
0 °C

実験手順

Under a nitrogen atmosphere, a 100-mL Schlenk flask was charged with 0.98 g (1.70 mmol) of cyclohexylidene(cyclopentadienyl)(2,7-diphenyl-3,6-ditert-butylfluorene) and 40 mL of dehydrated diethyl ether, and the mixture was stirred. This mixed slurry solution was cooled to 0° C. in an ice bath, and 2.40 mL (3.74 mmol) of a 1.56 mol/L hexane solution of n-butyllithium was added. The mixture was stirred for 23 hours while gradually warming to room temperature. This red reaction solution was cooled to −78° C. in a dry ice/methanol bath, and then 0.391 g (1.68 mmol) of zirconium tetrachloride was added. Subsequently, the mixture was stirred for 22 hours while gradually warming to room temperature to obtain an orange suspension. The solvent was removed by distillation under reduced pressure. Under a nitrogen atmosphere the residue was dissolved in n-hexane. The liquid was passed through a glass filter filled with Celite, and insolubles were washed with n-hexane, and the red powders insoluble in n-hexane was subjected to extraction with dichloromethane. The solvent in which the dichloromethane-solubles were dissolved was distilled off. The residue was washed with cold diethyl ether/cold n-hexane to obtain a target product as an orange solid (yield 0.71 g (57%)). The target product was identified by 1H-NMR and FD-MS spectroscopy.

後処理

  1. stirringThe mixture was stirred for 23 hours
  2. temperaturewhile gradually warming to room temperature
  3. temperatureThis red reaction solution was cooled to −78° C. in a dry ice/methanol bath
  4. stirringSubsequently, the mixture was stirred for 22 hours
  5. temperaturewhile gradually warming to room temperature
  6. customto obtain an orange suspension
  7. customThe solvent was removed by distillation under reduced pressure
  8. dissolutionUnder a nitrogen atmosphere the residue was dissolved in n-hexane
  9. filtrationfilter
  10. additionfilled with Celite, and insolubles
  11. washwere washed with n-hexane
  12. extractionthe red powders insoluble in n-hexane was subjected to extraction with dichloromethane
  13. dissolutionThe solvent in which the dichloromethane-solubles were dissolved
  14. distillationwas distilled off
  15. washThe residue was washed with cold diethyl ether/cold n-hexane

出典と根拠

ORDレコード
ord-c15cb12748f0418eaebf97cc0af20a9d
出典データセット
uspto-grants-2016_07
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US09382356B2

反応ノート

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