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Hydrochloric Acid → 3-Hydroxy-5-(pentafluorosulfanyl)benzoic acid

HRID 1055647
ノート
印刷プレビュー

反応式

HRID 1055647 の反応式
Br[C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([S:11]([F:16])([F:15])([F:14])([F:13])[F:12])[CH:10]=1)[C:5]([OH:7])=[O:6].C(P(C(C)(C)C)C1C=CC=CC=1C1C(C(C)C)=CC(C(C)C)=CC=1C(C)C)(C)(C)C.[OH-:47].[K+].Cl>O1CCOCC1.O.C1C=CC(/C=C/C(/C=C/C2C=CC=CC=2)=O)=CC=1.C1C=CC(/C=C/C(/C=C/C2C=CC=CC=2)=O)=CC=1.C1C=CC(/C=C/C(/C=C/C2C=CC=CC=2)=O)=CC=1.[Pd].[Pd]>[OH:47][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([S:11]([F:16])([F:15])([F:14])([F:13])[F:12])[CH:10]=1)[C:5]([OH:7])=[O:6]
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

8

反応物 4

HCID 313Hydrochloric AcidHCID 14797Potassium HydroxideHCID 11618717Di-tert-butyl(2',4',6'-tris(propan-2-yl)-(1,1'-biphenyl)-2-yl)phosphaneHCID 581374213-Bromo-5-(pentafluorosulfur)benzoic acid

生成物 1

HCID 581367943-Hydroxy-5-(pentafluorosulfanyl)benzoic acid

試薬・触媒・溶媒 3

HCID 9811564
Bis(dibenzylideneacetone)palladium
触媒
HCID 962Water溶媒
HCID 312751,4-Dioxane溶媒

反応条件

温度
100 °C

実験手順

2.0 g (6.11 mmol) of the compound of Example 15A were dissolved in 20 ml of dioxane and 2 ml of water, the mixture was degassed with argon, 280 mg (0.31 mmol) of tris(dibenzylideneacetone)dipalladium, 325 mg (0.76 mmol) of 2-di-tert-butylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl and 1.37 g (24.5 mmol) of powdered potassium hydroxide were added and the mixture was stirred at 100° C. for 2 h. The reaction was then stirred into 50 ml of 1 M hydrochloric acid and extracted twice with in each case 50 ml of ethyl acetate. The combined organic phases were washed with saturated sodium chloride solution, dried over sodium sulphate and concentrated under reduced pressure. The residue was suspended in dichloromethane/pentane (9:1), the solid was filtered off and the filter cake was dried under high vacuum. This gave 980 mg (59% of theory) of the title compound.

後処理

  1. additionwere added
  2. extractionextracted twice with in each case 50 ml of ethyl acetate
  3. washThe combined organic phases were washed with saturated sodium chloride solution
  4. dry with materialdried over sodium sulphate
  5. concentrationconcentrated under reduced pressure
  6. filtrationthe solid was filtered off
  7. customthe filter cake was dried under high vacuum

出典と根拠

ORDレコード
ord-2b287bdb33f7402dbf5e971fb5567daa
出典データセット
uspto-grants-2016_07
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US09394309B2

反応ノート

読み込み中…

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