Cyclobutylcarbinol → 4-Bromo-3-(cyclobutylmethoxy)-N-methyl-2-nitroaniline

HRID 1056963ノート

反応式

HRID 1056963 の反応式
[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1F.[CH:14]1([CH2:18][OH:19])[CH2:17][CH2:16][CH2:15]1>>[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1[O:19][CH2:18][CH:14]1[CH2:17][CH2:16][CH2:15]1

参加物

3

反応物 2

HCID 78130CyclobutylcarbinolHCID 1180938324-Bromo-3-fluoro-N-methyl-2-nitroaniline

生成物 1

HCID 1180938704-Bromo-3-(cyclobutylmethoxy)-N-methyl-2-nitroaniline

実験手順

This compound was synthesized according to the procedure of Example 11, Step 1, using 4-bromo-3-fluoro-N-methyl-2-nitroaniline and cyclobutylmethanol as the starting materials. LCMS calculated for C12H16BrN2O3 (M+H)+: m/z=315.0, 317.0. found: 315.0, 317.0.

後処理

  1. customThis compound was synthesized

出典と根拠

ORDレコード
ord-dae2fc49103a4fbfaf3109d5986073d2
出典データセット
uspto-grants-2016_07
特許番号
US09399640B2

反応ノート

読み込み中…