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HRID 10570作成日:2026年10月26日

Hydrochloride methanol → HCID 178418756、化合物

https://huagongshe.com/reaction/10570

反応式

関与物質

役割名称HCID仕込み量
反応物Hydrochloride methanolHCID 21893726—
反応物HCID 178418777HCID 178418777—
生成物HCID 178418756HCID 178418756—

反応手順

According to the method of Example 1, Step C, deprotection was performed (room temperature, 2 hours) by using Intermediate 124 (83.9 mg) and 10% hydrogen chloride/methanol solution (2 ml). The solvent was evaporated under reduced pressure, and the residue was added with methanol (0.5 ml) and diethyl ether (1.5 ml). The deposited precipitates were collected by filtration and washed with diethyl ether to obtain the title compound (63.3 mg).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07094789B2
出典データセットuspto-grants-2006_08
ORD IDord-98d12fb782ec41e3aba8ea2af660275d
出典メモuspto-grants-2006_08