Cyclohexanemethanol → 4-Bromo-3-(cyclohexylmethoxy)-N-methyl-2-nitroaniline

HRID 1057000ノート

反応式

HRID 1057000 の反応式
[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1F.[CH:14]1([CH2:20][OH:21])[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]1>>[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1[O:21][CH2:20][CH:14]1[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]1

参加物

3

反応物 2

HCID 7507CyclohexanemethanolHCID 1180938324-Bromo-3-fluoro-N-methyl-2-nitroaniline

生成物 1

HCID 1180939244-Bromo-3-(cyclohexylmethoxy)-N-methyl-2-nitroaniline

実験手順

This compound was synthesized according to the procedure of Example 11, Step 1, using 4-bromo-3-fluoro-N-methyl-2-nitroaniline and cyclohexanemethanol as the starting materials. LCMS calculated for C14H20BrN2O3 (M+H)+: m/z=343.1, 345.1. found: 343.0, 345.1.

後処理

  1. customThis compound was synthesized

出典と根拠

ORDレコード
ord-f282bd17319a4a07a980abc584e2a5d6
出典データセット
uspto-grants-2016_07
特許番号
US09399640B2

反応ノート

読み込み中…