Phenol → 4-Bromo-N-methyl-2-nitro-3-phenoxyaniline

HRID 1057020ノート

反応式

HRID 1057020 の反応式
[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1F.[C:14]1([OH:20])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[Br:1][C:2]1[CH:9]=[CH:8][C:5]([NH:6][CH3:7])=[C:4]([N+:10]([O-:12])=[O:11])[C:3]=1[O:20][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

参加物

3

反応物 2

HCID 996PhenolHCID 1180938324-Bromo-3-fluoro-N-methyl-2-nitroaniline

生成物 1

HCID 1180939434-Bromo-N-methyl-2-nitro-3-phenoxyaniline

実験手順

This compound was synthesized according to the procedure of Example 1, Step 1, using 4-bromo-3-fluoro-N-methyl-2-nitroaniline and phenol as the starting materials. LCMS calculated for C13H12BrN2O3 (M+H)+: m/z=323.0, 325.0. found: 322.9, 325.0.

後処理

  1. customThis compound was synthesized

出典と根拠

ORDレコード
ord-c1a0929503084d6a83700e700684d8be
出典データセット
uspto-grants-2016_07
特許番号
US09399640B2

反応ノート

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