化工社化工社 化学情報印刷レポート · 研究参考用
3,5,5-Trimethylhexanoic acid → n-(3,5,5-Trimethylhexanoyl)-2-octyldodecylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5,5-Trimethylhexanoic acid | HCID 90960 | — |
| 反応物 | 2-n-Octyl-1-dodecylamine | HCID 18761999 | — |
| 溶媒 | Heptane | HCID 8900 | — |
| 生成物 | n-(3,5,5-Trimethylhexanoyl)-2-octyldodecylamine | HCID 18673283 | 70.3% |
反応手順
3.6 g of 3,5,5-trimethylhexanoic acid and 6.8 g of 2-octyldodecylamine were mixed together in the tube of a microwave machine (Maxidigest™ MX 350 from the company Prolabo; frequency 2450±50 MHz, modulable power 300 W). After irradiation for about 50 minutes at 170° C.±10° C., the reaction mixture was dissolved in heptane and then purified on silica. 7 g of the desired amide were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06515178B2 |
| 出典データセット | uspto-grants-2003_02 |
| ORD ID | ord-1f2d4dd1ea454dd89335a466038b600c |
| 出典メモ | uspto-grants-2003_02 |