化工社化工社 化学情報印刷レポート · 研究参考用
Methyl bromoacetate → Methyl (2-formyl-4-methoxyphenoxy)acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl bromoacetate | HCID 60984 | — |
| 反応物 | 2-Hydroxy-5-methoxybenzaldehyde | HCID 95695 | — |
| 生成物 | Methyl (2-formyl-4-methoxyphenoxy)acetate | HCID 43212883 | 86% |
反応手順
In the same manner as in Reference Example 1, 5-methoxysalicylaldehyde was reacted with methyl bromoacetate to yield methyl 2-formyl-4-methoxyphenoxyacetate (yield 86%), which was then recrystallized from acetone-hexane to yield colorless prisms having a melting point of 74° to 75° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05723479 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-8d8d9084812145079c62beccf28cf5f0 |
| 出典メモ | uspto-grants-1998_03 |