化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Dibromobenzene → 1-(3-bromophenyl)-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Dibromobenzene | HCID 11414 | — |
| 反応物 | isopropyl(1-trityl-1H-imidazol-4-yl)ketone | HCID 10150490 | — |
| 生成物 | 1-(3-bromophenyl)-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanol | HCID 18668522 | 76.5% |
反応手順
By the reaction in the same manner as in Example 1-(ii) using 1-(1-trityl-1H-imidazol-4-yl)-2-methyl-1-propanone (34.90 g) and O-dibromobenzene (50.7 g), the title compound (37.7 g) was obtained as a colorless solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06518257B1 |
| 出典データセット | uspto-grants-2003_02 |
| ORD ID | ord-0b6183ee55c344d7991f677affe8a9c4 |
| 出典メモ | uspto-grants-2003_02 |