化工社化工社 化学情報印刷レポート · 研究参考用
Propan-2-yl 2,3,3,3-tetrafluoro-2-(heptafluoropropoxy)propanoate → (CF3)2Cfococf(CF3)ocf2CF2CF3
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propan-2-yl 2,3,3,3-tetrafluoro-2-(heptafluoropropoxy)propanoate | HCID 10177266 | — |
| 反応物 | (CF3)2Chococf(CF3)ocf2CF2CF3 | HCID 10277469 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | (CF3)2Cfococf(CF3)ocf2CF2CF3 | HCID 131724614 | — |
反応手順
Further, the same operation was repeated once. The total amount of benzene injected was 0.219 g, and the total amount of R-113 injected was 21 ml. Further, nitrogen was supplied for 1.5 hours. The product was quantified by 19F-NMR, whereby the yield of the above identified compound to (CH3)2CHOCOCF(CF3)OCF2CF2CF3, was 48.1%, and the yield of (CF3)2CHOCOCF(CF3)OCF2CF2CF3 to (CH3)2CHOCOCF(CF3)OCF2CF2CF3, was 19.1%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06969776B2 |
| 出典データセット | uspto-grants-2005_11 |
| ORD ID | ord-b79f83f57f5546bc90cfd9bd875c024e |
| 出典メモ | uspto-grants-2005_11 |